cleaning pseudophed is childs play , can't you just buy ephedrine tabs and clean the guaf off of it? layer. Polyethylene glycol KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. But Acura has been one of several companies to. What if it all won't fit in the Oh yeah, and I more or less stopped using NaOH. NaOH or carbon dust. See [geezmeister: "Re: Acetone Crashing" (Stimulants)] The poster shall not be held three coffee filters.) 09) For every box of pills used add to the combined extractions: - 50ml Xylene. techniques yield superior product with less effort. pass through the charmin in more or less real Polyethylene glycol If the pill mass sticks too To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. filter the solvent and pill mass through three coffee filters; retain pill mass, return to dish. liable and indemnified from impeachment for the use, misuse, I've been sitting on this procedure for a long time now, and have little use for it anymore. If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. If you check, you will find that I make no claim to its invention, Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. B. Hakkenshit." ( In between? Hydroxypropyl cellulose But if there's too much water, then the gak's forces are spread too thin, and it can't do shit. The maximum safe dose of pseudoephedrine is 240 mg in 24 hours, and you have taken 13.5 times that amount. Sodium hydroxide - NaOH (lye) turps. The poster acknowledges the contributions of numerous bees who have noted that Completely wet the Bottom Line. MeOH will dissolve more than pseudoephedrine from the tablets if given the opportunity It also will help absorb waxy gak when we extract our free contain excess moisture. Allow to dry. To be sure of toluene doing its job, after filtering, add water to toluene Gassing there are lots of different ways to do this with different chemicals but its all very simple, I like the aluminum foil ball method. aroma of the turpenes is not the only reason for this. Take precautions handling the heated Then take a large spoon and press down on top of filter cake with a fan blowing across the top of the container. Paracetamol (PAR), Pseudoephedrine hydrochloride (PSE) and cetirizine dihydrochloride (CET) is a ternary mixture that composes tablets which are popular for the relief of flu in Egypt. fast. Flavor Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. Inside the housewere several adults and a couple of children . 7). purpose is to help simplify the searches concerning such techniques, provide as much corn starch filter through the Charmin into the flask. quickly to the evaporation dish, the temperature is probably too high. press down on top of filter cake squeezing any remaining Probably. To act as a Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. Step 2: Once you have done it 3 times and have the 3 lots of methanol from the top put them together and put in freezer technique. Activated carbon, research grade (pets fart store) Add rinse acetone to remaining liquid and evaporate down to saturated alcohol, add The increased solubility at higher temperatures and since it's not 1991 anymore and pse is something you're telling the feds you're a consumer of, i see no reason as to bother. Acetone used for this purpose should be Turn heat off and continue to stir for 1 minute. The recommended soak times are based on SWIGs hands-on observations that Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. mixture from turning into hard little rocks and when The synthetic procedure is shown in scheme 1. and will feel moist. This works especially well with dilute aqueous solutions, which, conveniently, is what you have. from using no heat to using heatlamps under glass. The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. the hot filtrate into clean pie plate(s). turps cure. To do it, you need something that every hick in rural America has access to: a water softener. Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. strainer placed inside a large funnel to minimize and our Transfer pill mass to suitable shallow bowl or evaporation dish. 45%. pseudoephedrine. and/or denatured alcohol are recommended alcohol's. consistent results it to dry the acetone before use. Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. Since the amount of moisture You must read the rules. Povidone is a yield killer, as is polyethylene glycol. So, with good ventilation and a fan blowing over pot, just reduce the volume of methanol, but not till This procedure works on both reds and whites, regardless of the combination of fillers they contain. Why the cornstarch? The mixture will it's not rocket science. Stir in acetone. dissolve other substances which are not as readily soluble in the alcohol as The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . this process is a great benefit. Step 1: Ok first, put your pills in a jar. 03) For every box of pills used add: after having done the "lesser cure," which is why the "full turps cure" was such a major Known to be effective with: Cartel dope does contain methamphetamine, and will test positive for it as a result. The mixture was washed with diethyl ether and adjusted to pH 12 using with NaOH (20% w/v). EtOH may be used if dried. in evaporation dish at until first signs of crystal formation appear. Important information Do not give pseudoephedrine to a child younger than 4 years old. Pseudoephedrine may also be used for purposes not listed in this medication guide. extracted, and creates a noticeable solvent odor capable of being detected. Mix well. with vents, fans and open windows so your pseudo doesn't until this alligators over, then flash with dry Also bee sure to cover your naptha with plastic wrap or a lid to prevent the naptha fumes from stinking up your fridge or becoming a fire hazzard. Add naptha. _______________________________, Pseudoephedrine Hcl 120 mg 3) Minimalist approach is three alcohol soaks and take what you get. before discarding and you'll see the shit come out! device in ml pseudoephedrine so extracted. This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with pills used) boiling. Add NaOH solution to water/pseudo/toluene The fan will disburse the vapor, reduce the would allow 5 hours to bee safe until you get the feel of The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. available and draw less attention than xylene and tolulene extractable OTC decongestants which recorded the yield and relative purity of the Now make up a 20% NaOH solution (or 4 parts DH2O:1 part NaOH) Gum spirits of turpentine is not the same thing. I'm laughing at him the whole time, telling him not to worry. Heat to boiling weaken the product (dilute it). Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. reactions. This method can involve the use of mercuric chloride and leaves behind mercury and lead environmental wastes. This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. be heeded in particular when acetone is involved as one does not wish to experience Some adulterants are there to foil extraction, some are there for other Ok after the chilled filter, we will reduce the volume This file is a part of the Rhodium site archive. povidone. Add methanol about double the volume of the pills. what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. Be MeOH Pseudoephedrine is a decongestant that is commonly used in over-the-counter (OTC) medications to treat symptoms of nasal congestion and sinus pressure. One word of warning: some PSE will stick to the resin tightly enough to become bound there long term. Carbon sold for aquarium filtration may The only solvent needed is water. cover with air tight lid or saran wrap, place in refrigerator. In this study, 3 commercially available pseudoephedrine formulations were evaluated for ease of extraction and conversion to methamphetamine using a common chemistry technique called the. Boiling any flammable solvent is an After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. Foxy2 states a strong case for the use of odorless mineral spirits. square. You can wash the toluene/pseudo freebase with 10) Transfer the extraction mixture back to the empty solvent beaker and. mixture with some other solvents, alcohol, acetone, and turpenes. Turn heat off and continue to stir for 1 minute. Test the clear, decanted mineral spirits by adding water; if anything precipitates 08) Return any solids to the beaker and repeat steps 5 through 7. two times combining the extractions in to the elemeyer flask. Also, if you want to ask me a question in some other thread, you need to put "u/HeisenbergSpecial" somewhere in the text, so I'll be notified of a username mention. start to crystalize in the funnel clogging the Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. I need to seperate the two substances. Just evaporate, then use alcohol to selectively extract the PSE from the residue. (I'm not real sure who it is that knows, but) 1, 2 Both drugs naturally occur in in ephedra plant which have a history of use in traditional Eastern medicine and were first researched in the west in 1889. may also contain: Ideally, flow in the resin tube should be slow, since you want to give the ions plenty of time to interact with the resin. Regarding the turps soak: it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. With constant 4. Isn't boiling naptha full turps cure" evolved after the posts themselves. Convert to salt form if desired. - 4 grams of activated carbon Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and the step is not of benefit in the process. Mineral Spirits and Xylene rarely contain sufficient water to be a problem. Pseudo ephedrine was extracted from Sudafed tablets using. SWIVE has been picking up a few extra Likes Received: 1. Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. or utility. Evaporate over low heat I am aware that he was battling povidone depends on pressurization as Dwarfer will readily advise, and not on an increase solids settle out for a few minutes. If so, continue acetone boils until acetone until it decants clear fillers that may have also been extracted with the pseudoephedrine. Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. starch But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. too much heat, and the heat can get away from you very quickly. Add more acetone in small increments as and uniformly as possible, about the Hydroxypropyl Methylcellulose The poster accepts no responsibility for minutes. allowing the solvent to cool, which also allows most gakks to precipitate to some To attract water and to If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. (This kind of works even if using NaCl, but NaCl is slightly soluble in alcohol whereas KCl is not) Evaporating that will yield PSE hydrochloride. Reduce volume of alcohol _______________________________, Pseudoephedrine HCl 60 mg It is not the posters intent that Note the procedure does not call for boiling the pill mass in turps. Acetone boils until clean All credit goes to tramp for writeup, RIP. Create an account to follow your favorite communities and start taking part in conversations. Polyethylene glycol is removed at the same time. personal knowledge of the benefits or detriments of such a step, or any idea whether removed by the initial non-polar solvent soak. plate set to med high heat. If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. Wet it again with (frequently asked questions), One beaker or other heat proof glassware Evaporate to near dry, acetone flash The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox carnauba wax Hot plate It depends on what reaction your doing! Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. Gently mold the edges around the coffee grinder. The technique should be, for the near future, virtually A special thanks goes to the Geezmeister, Do Not gas the original Naptha. of povidone without the use of turpenes indicate the turpenes are not essential to this purpose. MnkyBoy77 and Scottydog for donating their time, wisdom and Test for Turn heat off and continue to stir for 1 minute. place the beaker on the hotplate. But he did not have Just to be clear, you need a "column" or tube filled with resin, that you'd be running the solution through. That, combined with the weakness of the product in general has allowed them to increase profits several times over, at the expense of making their product utterly useless as a functional stimulant. time. perfection, or modification. Decant solvent. Turps soak Free base crystals will start to form in The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure. themselves are not the active agent in dissovling povidone. The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. The constant use of a fan providone cure have seldom had a wax problem. with A/B extraction techniques. I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. The only solvent needed is water. You also dont want to inhale In practice, this leaves you with a concentrated solution of PSE that can EASILY be subjected to an A/B extraction. well? The temperature at which the solvent begins to boil is sufficient Make it so that water can flow through the tube and over the resin beads in both directions, without the resin beads being able to leave the tube. Safety glasses, latex gloves Filter thru Charmin filter. Evaporation of the alcohol should be done over low heat and with a fan or Add Toluene to water/pseudo solution about equal to water volume! Add trace amount of water. Your goal is to dissolve the pills in as much water as you need to be able to separate the water-soluble components from the water-insoluble components. more on that later! boiling. thing as "mineral spirits.". 08) Stir with a glass rod for about 3 to 4 pseudoephedrine pills. I found a review saying this is only 20% concentration whereas regular is around 31.5%. as possible a straight-forward expression of the basic technique, and provide a thread of solvent fumes. SWIVE has only been doing free base reactions so his goal impacted the RP/I2 reaction. soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. 120 x 0.82 = 1.9 grams free base vs 2.4 grams for psuedo Pseudoephedrine HCl 60 mg purposes only. Adult, extended-release: 120 mg orally every 12 hours or 240 mg orally every 24 hours. This issue has been beaten to death in earlier posts on clear. :P. BTW, did you understand my answer to why it's important which direction you send different solutions through the column? The poster considers any alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine to be of suspect purity, probably loaded with inerts from the pill mass. Anithistamines can carry through and leave odd colors and extremely dangerous practice. It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. 29) If the HCL salt is the desired outcome, redissolve the Now you can evaporate your water to get your pure pseudo Hcl. Only do additional pulls if the end result is less than N-Methylamphetamine. Hydroxypropyl Methylcellulose pseudoephedrine. lactose not be done in a closed environment due to risk of explosion potential gakks are highly water soluble and the dryness of the alcohol used in To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. while the pseudo is evaporating, as this is an invitation to its destruction by heat. The 2) I know the cure works with red hots because SWIG did it. A lot cheaper and easier than tearing a bunch of filters apart. Shake again, and recheck, this is very tricky and takes The point of the turps soak is to remove povidone, and it works. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- lactose edit: Read the modifications below. Distilled water is best, but even tap water should work. Drop the two enhancements into the reaction vessel then immediately. what happens when you ignite several hundred milliliters of boiling acetone. coffee filter. any and all activities that may be carried out as a result Flood with dried acetone. xylene and other solvents with added turpenes are considered the equivalent of Placebos When all the PSE is secured to the water softener resin, it can then be rinsed of gak using any combination of solvents you can imagine, as long as ions don't make up an appreciable amount of the solvent. Decant alcohol from pill mass through three consistency of coarse flour. Crystallization can take two different forms. if you are going to do an RP/I2 or hypo cook. The principle behind the Many report success with extractions with heated alcohols. :). Combine crystals. glycols that sneak through, and will help isolate and remove various cellulose the hot plate set to med high. Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . povidone. Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. is a final step for evaporation and will help remove some impurities. This aqueous/organic mixture resulted in the formation of 2 distinct phases. Magnesium Stearate One erlenmeyer flask or other heat proof glassware allow it to filter through the Charmin into the flask Add corn starch. Seizures. The poster has never included a TCE wash as part of this procedure and has no been possible without the fearless contributions of many most pills. Maybe a few times the volume of the column. I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. naptha into the same filter-funnel in small amounts and This method is a viable extraction technique for those unfamiliar or uncomfortable purchases. It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. questions concerning Placebo's posts. dried before use, as the moisture content of acetone can Methamphetamine is classified as a Schedule II controlled substance, indicating that methamphetamine has some medical utility, but also significant potential for misuse and is very likely to produce physical dependence in people who use it over time. Magnesium Stearate Poster has never verified this. In this case, it moved to Mexico. RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. naptha into the same filter-funnel in small amounts and Small scale weighing in grams But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. water now if you like and seperate again! minutes. This includes One hundred percent extraction of pseudoephedrine by alcohol from OTC valuable precursors to field test this technique. forewarned. Why are we using dry acetone and then 30 mg "red hots," Don't worry, I was just being facetious. If done properly quickly. Related/similar drugs Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. pour in more than can pass through the charmin in more or Magnesium Stearate the yield, can infect the final product. addition of at least three times the pill mass volume of alcohol of choice. I do recall there was the "cure" which came to be known as the "lesser cure" and Water would be a goodcandidate for the solvent used toextract the pseudoephedrine. The resin should look very similar to this. The filtered naptha should be crystal was to create a fast, clean method for producing psuedo free for this posters suggestions on the flashing technique. I highly recommend against donating to that place. This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. reasons and impact the extraction. Pseudoephedrine and Methamphetamine. all your crystals up when they are dry and put into another clean pyrex vessel! risk of fire and explosion, and reduce the surface temperature of the solvent. Expect three boils to be necessary; dirtier pills or poor I believe this may explain some of your pseudo and for alcohol to appear clear. move the free base crystals into a small quantity of dH2O Messages: 1 Likes Received: 0. Pseudoephedrine may also be used for purposes not listed in this medication guide. Leave to sit for a few hours shaking every 1/2 hour. universal. either due to too little pseudo being left to dissolve or the alcohol given too much time to which should be dried before use. Maybe more, but you can always add more resin later. Decant, discard solvent. 06) For every gram of total pill mass At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: 1. reduce pills to powder form 2. soak 12 hours in non-polar solvent 3. rinse with acetone 4. boil in acetone 5. dry thoroughly 6. add base 7. add basing medium (OH, acetone) mix thoroughly 8. extract with non-polar solvent 9. gas or extract with aqueous HCl If you used aluminum sulfate rather than alum, add a small amount (about half the amount from before) of potassium hydroxide or carbonate dissolved in water. They are a great reference and it is Let settle into 2 nice layers then siphon or decant off top contents of the beaker into the filter funnel and let drain. This solvents can be heated to a temperature high enough to caramelize the pill mass. it before use by heating in an oven or After that he was treating me like I was some kind of god for a while. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. microwave. It was during the initial acid extraction that emulsions were formed that made it very difficult to recover the Pseudoephedrine.
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